-ANAP-hydrochloride-LCMS-31189-MedChemExpress

MS Report from Instrument: LCMS-03 File ..ta\\2018\\20180620\\20180620-1\\SQS5384-039-1.D Tgt Mass (CHM): Injection Date : 20 Jun 18 9:41 am +0800 Seq. Line : 16 Sample Name : SQS5384-039-1 Location : P1-B-01 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\LCMS03\\Data\\2018\\20180620\\20180620-1\\1-POS-3MIN.M Analysis Method : D:\\LCMS03\\Data\\2018\\20180620\\20180620-1\\1-POS-3MIN.M Catalog No : HY-101937C Batch#31189 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 A, Sig=214,4 Ref=off10000.919500000.5 DAD1 B, Sig=254,4 Ref=offmAU20000.322100001.285mAU1.1901.2511.3761.69411.2851.522.5min1.6941.72211..7767381.1591.1911.2531.3781.4481.4811.5131.5661.6152.00600.5 ELS1 A, ELSD Signal0.390mV500250011.522.5min1.3562.6052.936minminmin00.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 7060000040000020000000.51 Ion 1, MSD1 1,Target Mass 0 +H Positive, EIC=0.7:1.70.050-0.05-0.100.511.3121.522.51.4011.5501.7031.51.77122.51.522.5 Integration Results for DAD1 A, Sig=214,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.92 0.02 10.33 7.96 0.65 159 1.19 0.02 2.13 1.73 0.13 233 1.25 0.01 0.57 0.70 0.04 273 1.28 0.01 1559.80 1583.75 98.47 273 1.38 0.02 0.93 0.94 0.06 273 1.69 0.02 10.27 10.18 0.65 186 Integration Results for DAD1 B, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.32 0.03 0.57 0.28 0.02 431 1.16 0.02 0.35 0.37 0.01 159 1.19 0.02 2.91 2.84 0.11 233 1.25 0.01 0.84 1.09 0.03 273 1.28 0.01 2642.47 2703.43 99.23 273 1.38 0.01 1.25 1.54 0.05 273 1.45 0.01 0.63 0.73 0.02 233 1.48 0.02 1.02 1.13 0.04 233LCMS-03 6/22/2018 9:11:29 AM SYSTEMPage1 of5MS Report from Instrument: LCMS-03 1.51 0.01 0.54 0.75 0.02 233 1.57 0.01 0.29 0.40 0.01 233 1.61 0.02 0.52 0.51 0.02 233 1.69 0.02 7.78 7.51 0.29 186 1.72 0.02 0.95 0.98 0.04 186 1.76 0.01 1.10 1.37 0.04 338 1.78 0.02 1.45 1.13 0.05 338 2.01 0.02 0.38 0.25 0.01 233 Integration Results for ELS1 A, ELSD Signal RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.39 0.20 13451.15 851.82 93.52 431 1.36 0.05 885.27 285.43 6.16 273 2.60 0.06 21.13 5.46 0.15 105 2.94 0.05 25.17 7.44 0.18 105 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.31 0.06 2131421.25 607064.50 87.47 273 1.40 0.04 44570.77 17078.97 1.83 702 1.55 0.06 54761.71 14922.56 2.25 233 1.70 0.04 79510.02 27844.73 3.26 186 1.77 0.05 126543.92 44913.48 5.19 338LCMS-03 6/22/2018 9:11:29 AM SYSTEMPage2 of5MS Report from Instrument: LCMS-03Ret. Time: 1.31 <<<< POSITIVE SPECTRA >>>> ES-API Positive17500015000012500010000075000567.250000250000100200300400500600700800900m/z274.1 ES-API Positive1200010000105.180006000400020000100200300400500600700800900m/z233.1701.5102.2141.1273.1419.0589.5588.5217.1239.2362.4703.5702.5273.1Ret. Time: 1.40130.1305.1274.1155.1186.1339.3391.3624.3679.6Ret. Time: 1.55 ES-API Positive100008000141.160004000223.1241.1163.1140.1339.2106.1191.0265.020000100200300400500600700800900m/z304.1413.2986.6516.2500600700800900m/z105.1233.1Ret. Time: 1.70 ES-API Positive233.118000160001400012000100006000400020000100200300400338.28000261.0279.1102.2142.1105.1186.1814.6838.5330.3226.1188.1301.0395.1LCMS-03 6/22/2018 9:11:29 AM SYSTEMPage3 of5986.7973.4MS Report from Instrument: LCMS-03Ret. Time: 1.77 ES-API Positive200001500012500100007500102.2352.1199.9261.1280.1234.1395.1142.2305.125000100200300400500600700800900m/z420.3544.25000515.3233.117500105.1338.2279.1LCMS-03 6/22/2018 9:11:29 AM SYSTEMPage4 of5MS Report from Instrument: LCMS-03 *** End of Report ***LCMS-03 6/22/2018 9:11:29 AM SYSTEMPage5 of5