MS Report from Instrument: LCMS-03 File ..\\Data\\20171219\\20171219\\CPK2017-D18-09736.D Tgt Mass (CHM): Injection Date : 19 Dec 17 7:05 pm +0800 Seq. Line : 121 Sample Name : CPK2017-D18-09736 Location : P2-C-02 Acq. Operator : ZLJ_587 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\LCMS03\\Data\\20171219\\20171219\\1-POS-3MIN.M Analysis Method : D:\\LCMS03\\Data\\20171219\\20171219\\1-POS-3MIN.M Catalog No : HY-13805 Batch#09736 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 A, Sig=214,4 Ref=off5001.5621.626250000.5 DAD1 B, Sig=2,4 Ref=offmAU1.51.6031.628200000.5 ELS1 A, ELSD SignalmV502500.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 7020000001000000000.511.5 Ion 302.8, MSD1 302.8,Target Mass 301.8 +H Positive, EIC=302.5:303.5200000100000000.511.522.5min Integration Results for DAD1 A, Sig=214,4 Ref=off1.72422.5min1.51.72522.5min111.697mAU1.8742.0762.2571.51.69722.5min1.7811.8742.0772.21.51.722.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.56 0.02 0.69 0.65 0.08 233 1.63 0.02 0.44 0.36 0.05 233 1.70 0.02 900.15 787.68 98.99 302 1.87 0.02 4.95 3.68 0. 233 2.08 0.02 2.78 2.34 0.31 233 2.26 0.02 0.31 0.25 0.03 105 Integration Results for DAD1 B, Sig=2,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.56 0.02 0.43 0.39 0.07 233 1.60 0.01 0.19 0.21 0.03 233 1.63 0.02 0.28 0.25 0.05 233 1.70 0.02 599.40 522.41 98.69 302 1.78 0.02 0.67 0.46 0.11 302 1.87 0.02 2.79 2.05 0.46 233 2.08 0.02 3.00 2.41 0.49 233 2.25 0.02 0.60 0.51 0.10 105LCMS-03 12/20/2017 11:59:35 AM ZLJ_587Page1 of4MS Report from Instrument: LCMS-03 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.72 0.06 9346291.00 2553137.75 100.00 302LCMS-03 12/20/2017 11:59:35 AM ZLJ_587Page2 of4MS Report from Instrument: LCMS-03Ret. Time: 1.72 <<<< POSITIVE SPECTRA >>>> ES-API Positive302.14000003000002000001000000100200300400500600700800900m/z305.1303.1304.1LCMS-03 12/20/2017 11:59:35 AM ZLJ_587Page3 of4MS Report from Instrument: LCMS-03 *** End of Report ***LCMS-03 12/20/2017 11:59:35 AM ZLJ_587Page4 of4
